Application of the Standards in the Planimetric Method

The planimetric method in NIS-Elements Grain Size Module (NGS) measures Grain Size values of a single phase material structure in accordance with the following standards as described:

ISO 643

NGS applies the paragraph C.3.3 that is an exact copy of the ASTM E112 – 13 procedure described below.

JIS-G-0551 (2013)

NGS applies the paragraph B.3.3 „Count Method“ that is an exact copy of the ASTM E112 – 13 procedure described below.

ASTM E112-13

NGS applies the paragraphs 11.1, 11.2 and 11.4

According to 11.1

for the planimetric procedure, NGS generates a circle of known area while the optical configuration should be set to reach at least 50 grains in the field and count the number of grains within this area. NGS does not block measurement if the amount of grains is lower. NGS keeps the value of the area as a MaskArea in [mm2].

According to 11.2

NGS counts separatelly the number of the grains completely inside within the known area and the number of grains intersected by the circumference of the area.

According to 11.4

NGS calculates:

Number of equivalent whole grains

N = 1 x (num fully inside) + 0.5 x (num intersected)

Actual number per square mm

NA = N / MaskArea

Grain Size

G = (3.321928 log10 NA ) – 2.954

NGS displays Grain Size G as the nearest norm value (0, 0.5, 1, 1.5…14.0)

E1382-97 (2015)

NGS applies the paragraphs 13.9, 14.2, 14.3

According to 13.9.1

NGS detects grains inside a measurement field, deletes all grains intersecting the test area border and measures the total area of all of the grains Agi within a field and counts the number of grains Ni.

According to 13.9.2

NGS calculates

The average area of the grains in the field

Ai = Agi / Ni

According to 13.9.3

This measurement should be repeated for n fields, at least 5x (NGS does not block measurement if the number of fields is lower).

NGS calculates the mean grain area: Ā = mean value of {A1, A2 ….} in mm2

According to 14.3

NGS calculates

Grain Size

G = (-3.3223 log10 Ā) – 2.955

NGS rounds off the value of G to the nearest tenth unit (not displayed nor reported).

According 14.2

NGS displays Grain Size G as the nearest norm value (0, 0.5, 1, 1.5…14.0)